Preparation of zirconium tungstate
1.. Impregnation method A certain amount of zrocl2.8h20 was dissolved in an appropriate amount of deionized water, and ammonia was added to form a hydrogel. The pH value was adjusted to 9.0. After being placed at room temperature for 12h, the precipitate was filtered and washed with deionized water to be chlorine-free (0.1 mol·L ~ AgN03 solution was used for detection). Then the filter cake was soaked in anhydrous ethanol and alcoholized for 12 h in a constant temperature drying [...]